2-[2-(4-Methylpiperazin-1-yl)ethyl]isoindoline-1,3-dione

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2-[2-(4-Methyl­piperazin-1-yl)eth­yl]iso­indoline-1,3-dione

In the title compound, C15H19N3O2, the piperazine ring adopts a chair conformation, with its N-C bonds in pseudo-equatorial orientations. The dihedral angle between the C atoms of the piperazine ring and the phthalamide ring system (r.m.s. deviaiton = 0.008 Å) is 89.30 (8)°. In the crystal, mol-ecules are linked by C-H⋯O hydrogen bonds, generating a three-dimensional network and aromatic π-π in...

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Crystal structure of 1-cyclopropyl-2-ethyl-5-fluoro-6- (4-methylpiperazin-1-yl)-1H-benzimidazole.

biological activities,1 and some of them are used as drugs.2,3 In previous studies,4,5 we reported on the synthesis and biological evaluation of 1,2,5(6)-trisubstituted benzimidazoles as antihistaminic and antimicrobial agents. The synthesis of ethyl 1-cyclopropyl-5-fluoro-6-(4-methylpiperazine-1-yl)-1H-benzimidazole-2-acetate (1) was performed according to reported methods.6,7 1-Cyclopropyl-2-...

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1-[2-(Benzyl­amino)-4-pyrid­yl]-2-(4-fluoro­phen­yl)ethane-1,2-dione

The crystal structure of the title compound, C(20)H(15)FN(2)O(2), contains two crystallographically independent mol-ecules, which are related by a pseudo-inversion center and linked into dimers via inter-molecular N-H⋯N hydrogen bonds. The 4-fluoro-phenyl ring of mol-ecule A makes dihedral angles of 17.17 (16) and 62.25 (15)°, respectively, with the phenyl and pyridine rings. The 4-fluoro-pheny...

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2-[1-(4-Ethoxy­phen­yl)-2-oxo-4-styryl­azetidin-3-yl]isoindoline-1,3-dione

The title compound, C(27)H(22)N(2)O(4), contains a nearly planar four-membered β-lactam ring, which makes dihedral angles of 74.64 (12), 1.70 (11) and 73.67 (12)° with the nine-membered ring system, the benzene ring and the phenyl ring, respectively. The crystal structure is stabilized by C-H⋯O and C-H⋯π inter-actions and a π-π inter-action [centroid-centroid distance = 3.4505 (19) Å] is also p...

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ژورنال

عنوان ژورنال: Acta Crystallographica Section E Structure Reports Online

سال: 2014

ISSN: 1600-5368

DOI: 10.1107/s1600536814002232